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Pincer-type linear nitrosyl Rh(I) complexes, Rh(PCPtBu)(NO)][BF4] (2) and [Rh(PCPtBuCH2)(NO)][BF4] (8), are reported (PCPtBu = 1,3-bis[(di-tert-butylphosphino)methyl]-2,4,6-trimethylbenzene). Complex ...

Rh(I) complexes of the electron-rich, bulky PNPtBu ligand readily undergo oxidation by silver salts to monomeric Rh(II) complexes. ... RhCl with AgOC(O)CF 3 led only to chloride abstraction, with no ...